The interior of the furnace is evacuated, then the furnace heaters are turned on to heat the alloy above its liquidus temperature. Next, the interior of the furnace is filled with argon gas at a pressure about 900 psi (approximately equal to 6.2 MPa) to force the molten alloy to infiltrate the preform.
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The crystals of 53 were pyrolyzed at 305-310 °C in a muffle furnace under a stream of nitrogen to give 30 in 48% yield. CH3O 50 51 52 Schemes. The Diels-Alder reaction of 3,6-dimethoxybenzocyclobutene 30 with some dienophiles was studied (Scheme 9).
COMPREHENSIVE STUDIES OF SOLID WASTE MANAGEMENT First and Second Annual Reports These interim reports (SW-Srg) on work performed under Research Grant No. EC-00260 (formerly successive Grant Nos. were UI-00547 and SW-00003) to the University of California were prepared by C. G. GOLUEKE and P. H. McGAUHEY and have been reproduced as received by the grantee.